Experiment 3Table/ chart/diagram/image is missing. gratify download the Word roll to view it. Hydrolysis of Methyl Salicylate Aim To produce salicylic grace via the hydrolysis of methyl salicylate under rudimentary conditions. Introduction Methyl Salicylate is a colourless liquid at populate temperature is a naturally occurring tangled found in pass green inunct utilise as a rubefacient in deep passion system liniments and in small amounts as a flavouring cistron at no to a greater extent than 0.04%. Salicylic acrid is a colorless microcrystalline organic fertiliser acid is wide utilize in organic synthesis and functions as a graft hormone. It is derived from the metabolism of salicin. It is issuedo known for its use in anti-acne treatments.
[ 2] Reflux was a heating attend to whereby vapours from the reception mixture were condensed and returned to their original flask. This condition that the reaction could be retained at the boiling augur of the declaration while the reply was not dis articulateed to the atmosphere. This was an in-chief(postnominal) rate in ensuring a higher yield of salicylic acid by ensuring that sodium salicylate, the compound formed after hydrolysis of NaOH was not poached off and lost as vapour. Suction filtration was used to collect the desired crystals for and in the recrystallisation procedure. emptiness filtration occurs alacritous than soberness filtration by lowering the air pressure in the flask, pulling the strive into the flask, speeding up the on the whole march of filtration. It ensured that crystals ere separated from peeing as much as possible, so that the crystals could dry faster and the melting points could be notice accurately in a shorter period of time. Recrystallisation was carried out in order to honk the salicylic acid crystals as the first batch of crystals produced contained many contaminants much(prenominal) as Cl- from the acidification previously carried out, resulting in impure salicylic... If you want to pack a full essay, order it on our website: Ordercustompaper.com
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